Lactic Acid → HCID 68124039, compound

HRID 258592Notes

Reaction equation

HRID 258592 reaction equation
[CH:1]1([CH3:13])[CH2:6][CH2:5][CH:4]([CH:7]([CH3:9])[CH3:8])[CH:3]([C:10](Cl)=[O:11])[CH2:2]1.[C:14]([OH:19])(=[O:18])[CH:15]([CH3:17])[OH:16]>O>[CH:1]1([CH3:13])[CH2:6][CH2:5][CH:4]([CH:7]([CH3:9])[CH3:8])[CH:3]([C:10]([O:16][CH:15]([CH3:17])[C:14]([OH:19])=[O:18])=[O:11])[CH2:2]1

Participants

4

Reactant 2

HCID 612Lactic AcidHCID 13734319Cyclohexanecarbonyl chloride, 5-methyl-2-(1-methylethyl)-

Product 1

HCID 68124039HCID 68124039, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

p-Menth-3-oyl chloride (2.0 g.) was stirred with lactic acid (20 ml.) at room temperature for 20 hours. The reaction product was then poured into water (600 ml.) and extracted twice with ether. The extracts were dried (CaCl2) and the solvent removed under reduced pressure to leave 2-(p-menth-3-oyloxy)propionic acid as an oily liquid.

Workup

  1. extractionextracted twice with ether
  2. dry with materialThe extracts were dried (CaCl2)
  3. customthe solvent removed under reduced pressure

Sources & evidence

ORD record
ord-118a9caeb4754ca298fc83637934746f
Source dataset
uspto-grants-1977_07
Patent number
US04033994

Reaction notes

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