Hydrochloric Acid → HCID 53840723, compound

HRID 258707Notes

Reaction equation

HRID 258707 reaction equation
Cl.[NH2:2][CH:3]([CH2:7][C:8]1[CH:9]=[CH:10][C:11]2[O:15][C:14](=[O:16])[NH:13][C:12]=2[CH:17]=1)[C:4]([OH:6])=[O:5].Cl.[CH3:19]O>>[CH3:19][O:5][C:4](=[O:6])[CH:3]([NH2:2])[CH2:7][C:8]1[CH:9]=[CH:10][C:11]2[O:15][C:14](=[O:16])[NH:13][C:12]=2[CH:17]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 70618768HCID 70618768, compound

Product 1

HCID 53840723HCID 53840723, compound

Procedure

The product from Example 1 (0.1 mole) is held at reflux in 1500 ml of methanol saturated with HCl gas for 6 hours. The alcoholic solution is evaporated to yield a product which is recrystallized from water or methanol:ether to yield the title compound.

Workup

  1. customThe alcoholic solution is evaporated
  2. customto yield a product which
  3. customis recrystallized from water or methanol

Sources & evidence

ORD record
ord-663abcc6deda4b7ebbcd681fa10d9759
Source dataset
uspto-grants-1977_07
Patent number
US04034100

Reaction notes

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