反应详情

温度

140 °C

To 157 g isodecyl alcohol in 200 ml xylene is added 117 g AA, 1.0 g HQ and 2.0Q PTSA. The reaction mixture is heated for 2 hrs. at reflux (140° C) while the water of reaction is collected (17 ml). The reaction mixture is cooled and the xylene removed under reduced pressure to give 250 g isodecyl acrylate. The analytical data for this acrylate is shown below.

1. temperatureThe reaction mixture is heated for 2 hrs
2. customis collected (17 ml)
3. temperatureThe reaction mixture is cooled
4. customthe xylene removed under reduced pressure