HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-Decylpiperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl 4-decylpiperazine-1-carboxylate | HCID 228932 | — |
| Product | 1-Decylpiperazine | HCID 230544 | — |
Reaction Steps
53.4 Grams of 1-ethoxycarbonyl-4-decylpiperazine is combined with 300 ml. of concentrated hydrochloric acid and refluxed with stirring under a nitrogen atmosphere for approximately 48 hours. After cooling to room terperature the solvents are removed under reduced pressure. The resulting solid is suspended in ethanol, filtered, and air-dried to yield 1-decylpiperazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036828 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-bd9b7411d6924eb29a953337af8e2986 |
| Source note | uspto-grants-1977_07 |