Hydrogen Peroxide → HCID 21423245, compound

HRID 259146Notes

Reaction equation

HRID 259146 reaction equation
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH:13]=[N:12][N:11]=[N:10]2)=[CH:5][CH:4]=1.[OH:14]O>C1C=CC=CC=1>[CH3:1][S:2]([C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH:13]=[N:12][N:11]=[N:10]2)=[CH:5][CH:4]=1)=[O:14]

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 21423234HCID 21423234, compound

Product 1

HCID 21423245HCID 21423245, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

1-[p-(Methylthio)phenyl]-1H-tetrazole (2 g.) and 0.9 ml. of 30% hydrogen peroxide were refluxed with stirring in benzene for 3 hours. The benzene was decanted and the precipitate washed with benzene and recrystallized from acetone, m.p. 175°-176° C.

Workup

  1. customThe benzene was decanted
  2. washthe precipitate washed with benzene
  3. customrecrystallized from acetone, m.p. 175°-176° C.

Sources & evidence

ORD record
ord-1514869dbb974d3caa28ba32077b6cf9
Source dataset
uspto-grants-1977_07
Patent number
US04036849

Reaction notes

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