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HRID259216

反应详情

EQUATION

反应方程式

HRID 259216 的结构方程式

REACTANTS

反应物

3
结构：CC=O
HCID177

Acetaldehyde

C2H4O

结构：NS(=O)(=O)N1CCOCC1
HCID276739

4-Morpholinesulfonamide

C4H10N2O3S

结构：c1ccc(OP(c2ccccc2)c2ccccc2)cc1
HCID11543680

Phenoxydiphenylphosphine

C18H15OP

PRODUCTS

生成物

1
结构：CC(NS(=O)(=O)N1CCOCC1)P(=O)(c1ccccc1)c1ccccc1
HCID21423545

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Clc1ccccc1
溶剂HCID7964

Chlorobenzene

C6H5Cl

PROCEDURE

实验过程

When a mixture of equimolar quantities of phenyl diphenylphosphinite, acetaldehyde, and morpholinosulfonylamine in chlorobenzene is treated by the procedure used in the preceding experiment, the product is a white solid, mp 215°-217° C., 31P nmr (DMSO-d6) -30.9 ppm.

WORKUP

后处理

  1. additionis treated by the procedure