HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → Diphenyl[1-(morpholinosulfonylamino)ethyl]phosphine oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 4-Morpholinesulfonamide | HCID 276739 | — |
| Reactant | Phenoxydiphenylphosphine | HCID 11543680 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | Diphenyl[1-(morpholinosulfonylamino)ethyl]phosphine oxide | HCID 21423545 | — |
Reaction Steps
When a mixture of equimolar quantities of phenyl diphenylphosphinite, acetaldehyde, and morpholinosulfonylamine in chlorobenzene is treated by the procedure used in the preceding experiment, the product is a white solid, mp 215°-217° C., 31P nmr (DMSO-d6) -30.9 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036913 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-869234e2f04f418e8a5656bf746628e4 |
| Source note | uspto-grants-1977_07 |