HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21423938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21423825 | HCID 21423825 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21423938 | HCID 21423938 | — |
Reaction Steps
1-[3'-n-dodecylthio-2'-hydroxypropyl]imidazole (1.63 g.) in 20 ml. of dichloromethane and 2 ml. of thionyl chloride are stirred for 2 hours at room temperature. Thereafter, the reaction mixture is evaporated to dryness to yield 1-[2'-chloro-3'-(n-dodecylthio)propyl]imidazole hydrochloride as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036974 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-80a8cdc913ff45e9b0fde9130ce02c9c |
| Source note | uspto-grants-1977_07 |