HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 21423889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 21423875 | HCID 21423875 | — |
| Product | HCID 21423889 | HCID 21423889 | — |
Reaction Steps
Oxalic acid is added dropwise to a stirred solution of 3.2 g. of 1-[2',3'-bis(cyclohexylthio)propyl]imidazole in 300 ml. of anhydrous ether until precipitation is complete. The product is filtered off, washed with ether, air dried and recrystallized from ethyl acetate to yield 1-[2',3'-bis(cyclohexylthio)propyl]imidazole oxalate, m.p. 85.5°-88.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036974 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-285fa3e8b6994c05a7dbc8d49a31c4f1 |
| Source note | uspto-grants-1977_07 |