HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54114920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 68120797 | HCID 68120797 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54114920 | HCID 54114920 | — |
Reaction Steps
1-[2'-(4"-chlorobenzylthio)-3'-(n-hexylthio)propyl]imidazole oxalate (2.3 g.) in 100 ml. of dichloromethane is shaken with excess potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed with water, dried over magnesium sulfate and evaporated to yield 1-[2'-(4"-chlorobenzylthio)-3'-(n-hexylthio)propyl]imidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036973 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-fc3e70c6709641aaa899f2c7629c1573 |
| Source note | uspto-grants-1977_07 |