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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 259281Generated: October 29, 2026

Nitric Acid → HCID 21423753, compound

https://huagongshe.com/reaction/259281

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNitric AcidHCID 944—
ReactantHCID 21423754HCID 21423754—
ProductHCID 21423753HCID 21423753—

Reaction Steps

Nitric acid (70%; d = 1.42) is added dropwise to a stirred solution of 2.0 g. of 1-[3'-isopropoxy-2'-(pentachlorophenylthio)propyl]imidazole in 30 ml. of anhydrous ether until precipitation was complete. The product was filtered off, washed with ether, air dried, and recrystallized from ethyl acetate to yield 1-[3'-isopropoxy-2'-(pentachlorophenylthio)propyl]imidazole nitrate.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04036973
Source datasetuspto-grants-1977_07
ORD IDord-29e2f054d865433092fea4e63110bd87
Source noteuspto-grants-1977_07