Acetyl chloride → beta-Phenylthioethyl acetate

HRID 259297Notes

Reaction equation

HRID 259297 reaction equation
[C:1](Cl)(=[O:3])[CH3:2].[C:5]1([S:11][CH2:12][CH2:13][OH:14])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>N1C=CC=CC=1>[C:1]([O:14][CH2:13][CH2:12][S:11][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 696852-(Phenylthio)ethanol

Product 1

HCID 4148467beta-Phenylthioethyl acetate

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Acetylchloride (7.9g), β-phenylthioethyl-alcohol (15.4g) and pyridine (9.5g) were treated according to Example 1. On fractionation, a fraction (17.5g), b.p. 76.0°-77.0° C./0.04mmHg, of β-phenylthioethyl acetate was obtained.

Sources & evidence

ORD record
ord-cb1c793b4a324c8d82bfe7bbe1d9163f
Source dataset
uspto-grants-1977_07
Patent number
US04036984

Reaction notes

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