HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → beta-Phenylthioethyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-(Phenylthio)ethanol | HCID 69685 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | beta-Phenylthioethyl acetate | HCID 4148467 | — |
Reaction Steps
Acetylchloride (7.9g), β-phenylthioethyl-alcohol (15.4g) and pyridine (9.5g) were treated according to Example 1. On fractionation, a fraction (17.5g), b.p. 76.0°-77.0° C./0.04mmHg, of β-phenylthioethyl acetate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036984 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-cb1c793b4a324c8d82bfe7bbe1d9163f |
| Source note | uspto-grants-1977_07 |