HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 21424093, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 21424035 | HCID 21424035 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21424093 | HCID 21424093 | — |
Reaction Steps
A solution of 200 g. of 1-[2-(1-adamantyl)-2-(2,4-dichlorobenzyloxy)ethyl]imidazole in 20 ml. ethyl acetate is acidified with etheral oxalic acid. The product which precipitates is filtered off and recrystallized from methanol/acetone to yield 1-[2-(1-adamantyl)-2-(2,4-dichlorobenzyloxy)ethyl]imidazole oxalate, decomp. 203.5°-205.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04036975 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-31fb16c42b2247e69b9846413cc7c63c |
| Source note | uspto-grants-1977_07 |