Potassium Carbonate → HCID 21424034, compound

Participants

Reaction Steps

A suspension of 1 g. of 1-[2-(1-adamantyl)-2-(3,4-dichlorophenylthio)ethyl]imidazole nitrate in 100 ml. of dichloromethane is treated with excess aqueous potassium carbonate until a pH of about 11 is obtained. Thereafter, the suspension is shaken until a solution is obtained. The organic phase is then separated, washed with water, dried over magnesium sulfate and evaporated to dryness to yield 1-[2-(1-adamantyl)-2-(3,4-dichlorophenylthio)ethyl]imidazole.

Provenance & Evidence