Sodium → HCID 53878484, compound

HRID 259444Notes

Reaction equation

HRID 259444 reaction equation
C[O-].[Na+].[Na].[CH3:5][O:6][C:7](=[O:26])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15](=[O:25])[CH2:16][CH2:17][C:18](=O)[CH:19]([O:22][CH3:23])[O:20][CH3:21]>CO>[CH3:5][O:6][C:7](=[O:26])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][C:14]1[C:15](=[O:25])[CH2:16][CH2:17][C:18]=1[CH:19]([O:22][CH3:23])[O:20][CH3:21]

Participants

5

Reactant 3

HCID 5360545SodiumHCID 10942334Sodium MethoxideHCID 53710769HCID 53710769, compound

Product 1

HCID 53878484HCID 53878484, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

To a solution of sodium methoxide in methanol, prepared from 0.52 g of sodium and 90 ml of methanol, were added 5.68 g of a mixture containing about 5.28 g of 13,13-dimethoxy-9,12-dioxotridecanoic acid methyl ester.

Sources & evidence

ORD record
ord-a7d4ad62c78c44d981cd3ea25dc98452
Source dataset
uspto-grants-1977_07
Patent number
US04038305

Reaction notes

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