HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 21421902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-Cyclohexyl acetonimine | HCID 138744 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 21421902 | HCID 21421902 | — |
Reaction Steps
139 parts of acetone cyclohexylimine and 111 parts of triethylamine are dissolved in 500 parts of carbon tetrachloride, and the whole reacted with 110 parts of phosgene as described in Example 1. 123 parts (61% of the theory) of N-isopropenyl-N-cyclohexylcarbamyl chloride is obtained having a boiling point of 85° C. at 0.01 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038311 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-8bf2c38194504ca5b24e8494e9436d4b |
| Source note | uspto-grants-1977_07 |