Phosgene → HCID 21421902, compound

HRID 259478Notes

Reaction equation

HRID 259478 reaction equation
[CH:1]1([N:7]=[C:8]([CH3:10])[CH3:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(N(CC)CC)C.[C:18](Cl)([Cl:20])=[O:19]>C(Cl)(Cl)(Cl)Cl>[C:8]([N:7]([CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)[C:18]([Cl:20])=[O:19])([CH3:10])=[CH2:9]

Participants

5

Reactant 3

HCID 6371PhosgeneHCID 8471TriethylamineHCID 138744N-Cyclohexyl acetonimine

Product 1

HCID 21421902HCID 21421902, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

139 parts of acetone cyclohexylimine and 111 parts of triethylamine are dissolved in 500 parts of carbon tetrachloride, and the whole reacted with 110 parts of phosgene as described in Example 1. 123 parts (61% of the theory) of N-isopropenyl-N-cyclohexylcarbamyl chloride is obtained having a boiling point of 85° C. at 0.01 mm.

Sources & evidence

ORD record
ord-8bf2c38194504ca5b24e8494e9436d4b
Source dataset
uspto-grants-1977_07
Patent number
US04038311

Reaction notes

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