Phosgene → 27676-61-5

HRID 259479Notes

Reaction equation

HRID 259479 reaction equation
[CH:1]([N:4]=[C:5]([CH3:7])[CH3:6])([CH3:3])[CH3:2].C(N(CC)CC)C.[C:15](Cl)([Cl:17])=[O:16]>C(Cl)Cl>[C:5]([N:4]([CH:1]([CH3:3])[CH3:2])[C:15]([Cl:17])=[O:16])([CH3:7])=[CH2:6]

Participants

5

Reactant 3

HCID 6371PhosgeneHCID 8471TriethylamineHCID 1378922-Propanamine, N-(1-methylethylidene)-

Product 1

HCID 2142189827676-61-5

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

99 parts of acetone isopropylimine and 94 parts of triethylamine are dissolved in 400 parts of methylene chloride, and the whole reacted with 120 parts of phosgene at a temperature of 30° to 40° C., as described in Example 1. After isolation, 131 parts (81% of the theory) of N-isopropenyl-N-isopropylcarbamyl chloride is obtained having a boiling point of 69° C. at 3 mm.

Sources & evidence

ORD record
ord-ce74260db5984f96846981140cc39aa4
Source dataset
uspto-grants-1977_07
Patent number
US04038311

Reaction notes

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