反应详情

A mixture of 700mg. of 2-(3-nitrophenyl)oxazolo[4,5-b]pyridine in 50 ml. of ethanol was hydrogenated over 150 mg. of 5% palladium-on-carbon catalyst. The catalyst was removed by filtration and the solvent was concentrated to dryness. The residue was recrystallized from chloroformpetroleum ether to give 2-(3-aminophenyl)oxazolo[4,5-b]pyridine, m.p. 179°-180.5° C.

1. additionA mixture of 700mg
2. customThe catalyst was removed by filtration
3. concentrationthe solvent was concentrated to dryness
4. customThe residue was recrystallized from chloroformpetroleum ether