HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloride hydrochloride → 5-Benzyloxycarbonyl-6-benzyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloride hydrochloride | HCID 19596036 | — |
| Reactant | HCID 23465916 | HCID 23465916 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 5-Benzyloxycarbonyl-6-benzyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine | HCID 21325973 | 53% |
Reaction Steps
Obtained according to a procedure analogous to that of Example 7, from 5-carboxy-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine (Example 6) and benzyl chloride. Hydrochloride: pale yellow crystals; M.p. 135°-140° C. (isopropanol); Yield: 53%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04147787 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-b671f540aa9b4a5aa48ac542def02e55 |
| Source note | uspto-grants-1979_04 |