HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 2-(2-Benzoylaminophenyl)oxazolo[5,4-b]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2-(2-Aminophenyl)oxazolo[5,4-b]pyridine | HCID 12461421 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-(2-Benzoylaminophenyl)oxazolo[5,4-b]pyridine | HCID 22754783 | — |
Reaction Steps
An ice cold solution of 1 gram of 2-(2-aminophenyl)oxazolo[ 5,4-b]pyridine in 15 ml. of dry pyridine was treated with 1 gram of benzoyl chloride slowly. The reaction mixture was diluted with ice-water and stirred for 10 minutes and the resulting solid was collected on a filter and recrystallized from benzene to give 2-(2-benzoylaminophenyl)oxazolo[ 5,4-b]pyridine, m.p. 197°-198° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038396 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-721068ad9f0041479242c01e6ab4a900 |
| Source note | uspto-grants-1977_07 |