HRID259574

反应详情

EQUATION

反应方程式

HRID 259574 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2,5-Dimethyl-3-nitrobenzoic acid (10.0 g.) was hydrogenated in 200 ml. of methanol in the presence of 0.5 g. of 5% palladium on carbon. The catalyst was removed on a filter and the filtrate was concentrated to dryness to give 8.3 g. of 3-amino-2,4-dimethylbenzoic acid, m.p. 145.5°-146.5° C.

WORKUP

后处理

  1. customThe catalyst was removed on
  2. filtrationa filter
  3. concentrationthe filtrate was concentrated to dryness
  4. customto give 8.3 g