HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-dimethyl-3-nitrobenzoic acid → Benzoic acid, 3-amino-2,5-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-dimethyl-3-nitrobenzoic acid | HCID 257257 | — |
| Reactant | HCID 22754770 | HCID 22754770 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Benzoic acid, 3-amino-2,5-dimethyl- | HCID 43471 | — |
Reaction Steps
2,5-Dimethyl-3-nitrobenzoic acid (10.0 g.) was hydrogenated in 200 ml. of methanol in the presence of 0.5 g. of 5% palladium on carbon. The catalyst was removed on a filter and the filtrate was concentrated to dryness to give 8.3 g. of 3-amino-2,4-dimethylbenzoic acid, m.p. 145.5°-146.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038396 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-aa80e2321f354f44b67e1267e5ee2726 |
| Source note | uspto-grants-1977_07 |