HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 54318792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | HCID 54102988 | HCID 54102988 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 54318792 | HCID 54318792 | — |
Reaction Steps
Analogously to the description in Example 2, 2.5 g (0.01 mol) of 1-[p-(2-ethoxycarbonylaminovinyl)-phenoxy]-2,3-epoxy-propane, on reaction with 1.0 ml (0.01 mol) of tert.-butylamine in 50 ml of isopropanol, yield 1-[p-(2-carbethoxyaminovinyl)-phenoxy]-2-hydroxy-3-tertiary-butylaminopropane as an oil. Its N-cyclohexyl-sulphamate, prepared in acetone, shows a melting point of 99°-100° C. (from ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04038414 |
| Source dataset | uspto-grants-1977_07 |
| ORD ID | ord-2fdaa51bcc1e4fce9c53b97f5573e88b |
| Source note | uspto-grants-1977_07 |