Hydrochloric Acid → HCID 12439634, compound

HRID 259630Notes

Reaction equation

HRID 259630 reaction equation
[CH:1]([N:4]1[C:8](=[O:9])[CH2:7][CH2:6][C:5]1=[O:10])=[CH:2][CH3:3].[ClH:11]>>[Cl:11][CH:1]([N:4]1[C:8](=[O:9])[CH2:7][CH2:6][C:5]1=[O:10])[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 70588025HCID 70588025, compound

Product 1

HCID 12439634HCID 12439634, compound

Procedure

Anhydrous hydrogen chloride is bubbled through a mixture of 10 g. (0.072 mole) of N-propenylsuccinimide and 1.04 g. of stannic chloride for 6 hours. The solution is allowed to stand at room temperature for 10 days, the solution being saturated again with hydrogen chloride gas after 3 days and 4 days. Solvents are removed under reduced pressure at 30° - 40° C. to give 1-chloro-1-succinimidopropane as a yellow oil.

Workup

  1. customAnhydrous hydrogen chloride is bubbled through a mixture of 10 g
  2. customSolvents are removed under reduced pressure at 30° - 40° C.

Sources & evidence

ORD record
ord-7031570360ce4610978e77f506271beb
Source dataset
uspto-grants-1977_07
Patent number
US04038411

Reaction notes

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