HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 531871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 4-Ethylbenzoyl chloride | HCID 85368 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 531871 | HCID 531871 | 96.7% |
Reaction Steps
To a cooled solution of 9.6 g (0.11 mole) of morpholine in 25 ml methylene chloride is added 8.4 g (0.05 mole) of 4-ethylbenzoyl chloride dropwise. The reaction is stirred 30 minutes and a white precipitate formed. The mixture is washed three times each with 25 ml of water, dried over anhydrous magnesium sulfate and evaporated in vacuo to yield 10.6 g of yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523325 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-cb4cfa8b72e240b3873f9a45f4650b03 |
| Source note | uspto-grants-1996_06 |