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HRID259801

反应详情

EQUATION

反应方程式

HRID 259801 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(Cl)C(C)=O
HCID107332

Butanoic acid, 2-chloro-3-oxo-, methyl ester

C5H7ClO3

结构：CC(=O)[O-].[NH4+]
HCID517165

Ammonium acetate

C2H7NO2

PRODUCTS

生成物

1
结构：COC(=O)C(Cl)=C(C)N
HCID76224675

未命名化合物

收率 63.9%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

50 g (0.33 mol) of methyl 2-chloroacetoacetate are reacted with 64 g (0.83 mol) of ammonium acetate in 100 ml of methanol and worked up in analogy to Example 2. Yield: 63.9% [GC]