HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Acetate → HCID 86749530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | Ethyl 2-chloro-3-oxohexanoate | HCID 11424094 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86749530 | HCID 86749530 | 95.5% |
Reaction Steps
61.5 g (0.32 mol) of ethyl 2-chloro-3-oxohexanoate are reacted with 61.5 g (0.80 mol) of ammonium acetate in 120 ml of methanol and worked up in analogy to Example 2. Yield: 95.5% [GC]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523404 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-0508aa954e8844edb27f0e19dadcec43 |
| Source note | uspto-grants-1996_06 |