Ammonium Acetate → HCID 86749530, compound

HRID 259802Notes

Reaction equation

HRID 259802 reaction equation
[Cl:1][CH:2]([C:8](=O)[CH2:9][CH2:10][CH3:11])[C:3]([O:5][CH2:6][CH3:7])=[O:4].C([O-])(=O)C.[NH4+:17]>CO>[NH2:17][C:8]([CH2:9][CH2:10][CH3:11])=[C:2]([Cl:1])[C:3]([O:5][CH2:6][CH3:7])=[O:4]

Participants

4

Reactant 2

HCID 517165Ammonium AcetateHCID 11424094Ethyl 2-chloro-3-oxohexanoate

Product 1

HCID 86749530HCID 86749530, compoundYield 95.5%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

61.5 g (0.32 mol) of ethyl 2-chloro-3-oxohexanoate are reacted with 61.5 g (0.80 mol) of ammonium acetate in 120 ml of methanol and worked up in analogy to Example 2. Yield: 95.5% [GC]

Sources & evidence

ORD record
ord-0508aa954e8844edb27f0e19dadcec43
Source dataset
uspto-grants-1996_06
Patent number
US05523404

Reaction notes

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