HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formamide → HCID 178518080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formamide | HCID 713 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 86749532 | HCID 86749532 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178518080 | HCID 178518080 | — |
Reaction Steps
45.73 g (0.20 mol) of ethyl 3-amino-2-chloro-3-phenyl-propenoate are reacted with 31.9 g (0.71 mol) of formamide and 93 ml of sodium methylate solution in 120 ml of methanol and worked up in analogy to Example 9 (reaction time 16 h). Yield: 32.9 g (79.7%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05523404 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-1c15415382f14807bef38fd57aead757 |
| Source note | uspto-grants-1996_06 |