HRID260020

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID144686

Bicyclo[3.2.1]octane-2,4-dione

C8H10O2

结构：CS(=O)(=O)c1ccc(C(=O)Cl)c([N+](=O)[O-])c1

HCID14800186

4-(Methanesulfonyl)-2-nitrobenzoyl chloride

C8H6ClNO5S

PRODUCTS

生成物

结构：CS(=O)(=O)c1ccc(C(=O)C2C(=O)C3CCC(C3)C2=O)c([N+](=O)[O-])c1

HCID15790800

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

To a solution of 10 g of bicyclo[3.2.1]octane-2,4-dione in 100 ml of dichloromethane was added dropwise 70 ml of a dichloromethane solution having dissolved therein 19.1 g of 2-nitro-4-methylsulfonylbenzoyl chloride while ice cooling.

WORKUP

后处理

dissolutionhaving dissolved