HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20322477, compound → HCID 21325983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20322477 | HCID 20322477 | — |
| Reactant | 4-(4Chlorophenyl)-1-piperazinyl-ethanol | HCID 53901706 | — |
| Reactant | 3-(4-Chlorobenzoyl)-benzeneacetic acid chloride | HCID 54245591 | — |
| Product | HCID 21325983 | HCID 21325983 | — |
Reaction Steps
Using the procedure of Example 2, 3-(4-chlorobenzoyl)-benzeneacetic acid chloride was reacted with 4-(4chlorophenyl)-1-piperazinyl-ethanol to obtain 2-[4-(4-chlorophenyl)-1-piperazinyl]-ethyl 3-(4-chlorobenzoyl)-benzeneacetate with an Rf=0.68 (9-1-0.05 benzene-ethyl acetate-triethylamine eluant). Treatment with hydrochloric acid resulted in the formation of the hydrochloride salt melting at 142° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04147790 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-e4c2d7d7e62341cbbaba76a23b2d8d9c |
| Source note | uspto-grants-1979_04 |