HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrakis(diethylamino)zirconium → HCID 22401088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrakis(diethylamino)zirconium | HCID 139603 | — |
| Reactant | HCID 17763021 | HCID 17763021 | — |
| Product | HCID 22401088 | HCID 22401088 | — |
Reaction Steps
Bis(indenyl)ethane (0.327 g, 1.27 mmole) were reacted with zirconium tetra(diethyl amide) (1.025 g, 2.70 mmole, 6% excess for 1:2 stoichiometry) at 125° C. for 21/2 hours under nitrogen. This resulted in a light orange-yellow oil: 0.427 g of it were dissolved in 25 ml hexanes (46.1 mmole Zr/ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05527752 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-7602ed875a734daa958d08691105491a |
| Source note | uspto-grants-1996_06 |