HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropropionyl chloride → 3-Chloro-1-(2-oxo-1,2,2a,3,4,5-hexahydrobenz[cd]indol-6-yl)-1-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Reactant | 2a,3,4,5-Tetrahydrobenzo[cd]indol-2(1H)-one | HCID 599375 | — |
| Product | 3-Chloro-1-(2-oxo-1,2,2a,3,4,5-hexahydrobenz[cd]indol-6-yl)-1-propanone | HCID 15296944 | — |
Reaction Steps
Using 2a,3,4,5-tetrahydrobenz[cd]indol-2(1H)-one and 3-chloropropionyl chloride, the same procedure as in Reference Example 2 was followed, to yield the title compound as a colorless needle crystal having a melting point of 175° to 178° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05527800 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-3fb41dddd3f649798c7ec5da91331f3d |
| Source note | uspto-grants-1996_06 |