Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21463171 | HCID 21463171 | — |
| Product | HCID 21463115 | HCID 21463115 | — |
Reaction Steps
A mixture of the compound (4.7 g) obtained in Step 1, acetic acid (150 ml) and hydrochloric acid (150 ml) was heated for 7 hours at 110° C. The solvent was distilled off. To the residue was added ethyl acetate, which was washed with water and dried (MgSO4), then the solvent was distilled off to leave the title compound as colorless crystals (3.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05527811 |
|---|
| Source dataset | uspto-grants-1996_06 |
|---|
| ORD ID | ord-6f3cfaa10d444bd880f6a3a330145591 |
|---|
| Source note | uspto-grants-1996_06 |
|---|
