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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 260466Generated: October 30, 2026

3-Furoic acid → HCID 10487090, compound

https://huagongshe.com/reaction/260466

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Furoic acidHCID 10268—
ReactantBenzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphateHCID 151348—
ReactantHCID 18768729HCID 18768729—
ProductHCID 10487090HCID 10487090—

Reaction Steps

The title compound was prepared from furan-3-carboxylic acid (3.4 g, 0.030 mol), N,O-dimethylhydroxylamine hydrochloride hydrochloride (2.9 g, 0.030 mol) triethylamine (8.3 mL, 0.060 mol) and benzotriazol-1-yloxytris(dimethylamino)phosphonium hexafluorphosphate (13.3 g, 0.030 mol) according to the general procedure described in Example 1 for N-(3-pyridylmethyl)-5-chloro-3-phenylthio-2-carboxamide. NMR (DMSO-d6) δ8.25 (1H, s), 7.75 (1H, s), 3.70 (3H, s), 3.22 (3H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05527819
Source datasetuspto-grants-1996_06
ORD IDord-78fea008a4e8446c992ad7cc8e014f5c
Source noteuspto-grants-1996_06