HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → HCID 18421356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18421356 | HCID 18421356 | — |
Reaction Steps
In a 100 milliliter (hereinafter abbreviated to "mL") autoclave were placed 27.2 g of methyl methacrylate, 15.3 g of trimethylamine and 40 g of methanol under heating and shaking. After the temperature inside the autoclave reached 170° C., the reaction was continued at 170° C. for 3 hours. Upon completion of the reaction, the content in the autoclave was cooled, brought back to atmospheric pressure and analyzed. As a result, tetramethylammonium methacrylate was obtained in a yield of 76 mol % (based on trimethylamine).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05527927 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-82fdc6a5b24f4351943f5a7a374959a0 |
| Source note | uspto-grants-1996_06 |