Trimethylamine → HCID 18421356, compound

HRID 260541Notes

Reaction equation

HRID 260541 reaction equation
[C:1]([O:6]C)(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH3:8][N:9]([CH3:11])[CH3:10]>CO>[C:1]([O-:6])(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH3:8][N+:9]([CH3:1])([CH3:11])[CH3:10]

Participants

4

Reactant 2

HCID 1146TrimethylamineHCID 6658Methyl Methacrylate

Product 1

HCID 18421356HCID 18421356, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

In a 100 milliliter (hereinafter abbreviated to "mL") autoclave were placed 27.2 g of methyl methacrylate, 15.3 g of trimethylamine and 40 g of methanol under heating and shaking. After the temperature inside the autoclave reached 170° C., the reaction was continued at 170° C. for 3 hours. Upon completion of the reaction, the content in the autoclave was cooled, brought back to atmospheric pressure and analyzed. As a result, tetramethylammonium methacrylate was obtained in a yield of 76 mol % (based on trimethylamine).

Workup

  1. temperatureunder heating
  2. customreached 170° C.
  3. customUpon completion of the reaction
  4. temperaturethe content in the autoclave was cooled

Sources & evidence

ORD record
ord-82fdc6a5b24f4351943f5a7a374959a0
Source dataset
uspto-grants-1996_06
Patent number
US05527927

Reaction notes

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