反应详情

To a solution of (α-chloroethyl)chloroethylmethylsilane (0.171 g, 1 mmol) in diethyl ether (5 ml) was added a solution of benzylmagnesium bromide (1 mmol, 1 eq). The mixture was refluxed for 12 hours, then filtered. The product was purified by distillation.

1. temperatureThe mixture was refluxed for 12 hours
2. filtrationfiltered
3. distillationThe product was purified by distillation