HuagongsheHuagongshe Chemistry Print Report · For research reference only
(alpha-Chloroethyl)chloroethylmethylsilane → (alpha-Chloroethyl)benzylethylmethylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (alpha-Chloroethyl)chloroethylmethylsilane | HCID 123357515 | — |
| Reactant | HCID 178419663 | HCID 178419663 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | (alpha-Chloroethyl)benzylethylmethylsilane | HCID 123910545 | — |
Reaction Steps
To a solution of (α-chloroethyl)chloroethylmethylsilane (0.171 g, 1 mmol) in diethyl ether (5 ml) was added a solution of benzylmagnesium bromide (1 mmol, 1 eq). The mixture was refluxed for 12 hours, then filtered. The product was purified by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05529988 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-9027fb34faba4bf8a7bc0a5171441445 |
| Source note | uspto-grants-1996_06 |