Hydrochloric Acid → HCID 22399715, compound

HRID 260645Notes

Reaction equation

HRID 260645 reaction equation
[ClH:1].C(OC([NH:9][CH:10]([Si:18]([CH3:21])([CH3:20])[CH3:19])[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=O)(C)(C)C>C(OCC)C>[ClH:1].[CH3:20][Si:18]([CH3:19])([CH3:21])[CH:10]([NH2:9])[CH2:11][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22399693HCID 22399693, compound

Product 1

HCID 22399715HCID 22399715, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

A 3N solution of HCl in diethyl ether (3 ml) was added at room temperature to a mixture of N-tertbutoxycarbonyl-α-(trimethylsilyl)benzeneethanamine (0.150g, 0.51 mmol) in diethyl ether (3 ml). The mixture was stirred at room temperature for 48 hours. The resulting solid was filtered off and dried, in vacuo, to yield 0.106 g of the expected α-(trimethylsilyl)-benzeneethanamine hydrochloride,

Workup

  1. filtrationThe resulting solid was filtered off
  2. customdried, in vacuo

Sources & evidence

ORD record
ord-99b7049cf1f941c689e9f06d1badad68
Source dataset
uspto-grants-1996_06
Patent number
US05529988

Reaction notes

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