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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 260721Generated: October 29, 2026

Monobasic potassium phosphate → HCID 22400572, compound

https://huagongshe.com/reaction/260721

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMonobasic potassium phosphateHCID 516951—
ReactantPotassium FluorideHCID 522689—
ReactantHCID 22400569HCID 22400569—
SolventMethanolHCID 887—
ProductHCID 22400572HCID 22400572—

Reaction Steps

444 mg of potassium fluoride were added at ambient temperature to 500 mg of the product of Stage B in 5 ml of methanol. The reaction mixture was stirred for 3 hours, poured into 25 ml of an aqueous solution of potassium acid phosphate. Extraction was carried out with ethyl ether and the extracts were dried and the solvent was evaporated to obtain 360 mg of the expected product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05530022
Source datasetuspto-grants-1996_06
ORD IDord-30472fd50ac342ce8542a5a8e921f15e
Source noteuspto-grants-1996_06