Monobasic potassium phosphate → HCID 22400572, compound

HRID 260721Notes

Reaction equation

HRID 260721 reaction equation
[F-].[K+].[CH3:3][C:4]([O:19][Si](C)(C)C)([C:15]([F:18])([F:17])[F:16])[CH2:5][CH:6]1[CH:8]([C:9]([O:11][CH3:12])=[O:10])[C:7]1([CH3:14])[CH3:13].OP([O-])(O)=O.[K+]>CO>[CH3:3][C:4]([OH:19])([C:15]([F:18])([F:17])[F:16])[CH2:5][CH:6]1[CH:8]([C:9]([O:11][CH3:12])=[O:10])[C:7]1([CH3:13])[CH3:14]

Participants

5

Reactant 3

HCID 516951Monobasic potassium phosphateHCID 522689Potassium FluorideHCID 22400569HCID 22400569, compound

Product 1

HCID 22400572HCID 22400572, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

444 mg of potassium fluoride were added at ambient temperature to 500 mg of the product of Stage B in 5 ml of methanol. The reaction mixture was stirred for 3 hours, poured into 25 ml of an aqueous solution of potassium acid phosphate. Extraction was carried out with ethyl ether and the extracts were dried and the solvent was evaporated to obtain 360 mg of the expected product.

Workup

  1. extractionExtraction
  2. customthe extracts were dried
  3. customthe solvent was evaporated

Sources & evidence

ORD record
ord-30472fd50ac342ce8542a5a8e921f15e
Source dataset
uspto-grants-1996_06
Patent number
US05530022

Reaction notes

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