HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromomethylpropionate → 4-methoxybenzyl (E)-4-[3-[4-[1-(4-isobutylphenyl)pentyloxy]-2-butenoyl]1-indolyl]butyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromomethylpropionate | HCID 6993658 | — |
| Reactant | 3-Heptanoylindole | HCID 22400458 | — |
| Reactant | 4-Methoxybenzyl 4-bromobutyrate | HCID 22400462 | — |
| Reactant | (E)-3-[4-[1-(4-isobutylphenyl)pentyloxy]-2-butenoyl]indole | HCID 22400532 | — |
| Product | 4-methoxybenzyl (E)-4-[3-[4-[1-(4-isobutylphenyl)pentyloxy]-2-butenoyl]1-indolyl]butyrate | HCID 86749586 | — |
Reaction Steps
The procedure of Ex. 1 was repeated except that (E)-3-[4-[1-(4-isobutylphenyl)pentyloxy]-2-butenoyl]indole obtained in Step 4 of Pre. Ex. 19 was used in place of 3-heptanoylindole, and 4-methoxybenzyl 4-bromobutyrate obtained in Step 5 of Pre. Ex. 19 was used in place of 4-bromobutyrate to give 4-methoxybenzyl (E)-4-[3-[4-[1-(4-isobutylphenyl)pentyloxy]-2-butenoyl]1-indolyl]butyrate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05530019 |
| Source dataset | uspto-grants-1996_06 |
| ORD ID | ord-8f199d4c2ddc47aeae693f74e8f60d27 |
| Source note | uspto-grants-1996_06 |