HuagongsheHuagongshe Chemistry Print Report · For research reference only
Naphthalene → Naphthalene sodium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Naphthalene | HCID 931 | — |
| Reactant | 2,4,6-Trichloroaniline | HCID 12471 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Naphthalene sodium | HCID 66588811 | — |
Reaction Steps
Sodium naphthalene was prepared from naphthalene (12.8 g., 0.1 mole), sodium (2.3 g., 0.1 g atom) and tetrahydrofuran (200 ml.). Thereafter, 2,4,6-trichloroaniline (19.6 g., 0.1 mole) was added under nitrogen at ice bath temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163659 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-b371c0a792f44983bf447eed26baf14e |
| Source note | uspto-grants-1979_08 |