HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenol → HCID 12772646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | 4-Chloro-2,6-bis(hydroxymethyl)phenol | HCID 86914 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12772646 | HCID 12772646 | — |
Reaction Steps
A mixture of 4-chloro-2,6-bis(hydroxymethyl)phenol (4.8 g), 4-fluorophenol (16.0 g), benzene (25 ml) and hydrochloric acid (5 drops) was heated on a boiling water bath until all the benzene had evaporated. On cooling the mixture deposited colourless crystals of 4-chloro-2,6-bis(5-fluoro-2-hydroxybenzyl)phenol (11.9 g), mp 228° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163801 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-87520f8986e24a8ea199f6d604d28991 |
| Source note | uspto-grants-1979_08 |