HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 13064236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 5251690 | HCID 5251690 | — |
| Product | HCID 13064236 | HCID 13064236 | — |
Reaction Steps
A mixture of 2,6-bis(3-bromo-5-chloro-2-hydroxybenzyl)-4-fluorophenol (10 g), potassium carbonate (10 g) and dimethyl sulphate (7 g) in acetone (250 ml) was heated under reflux for 12 hr. The title compound was isolated and purified by column chromatography; m.p. c. 75°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04163801 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-54b52bf9fcbc40ac8f6f40446df0e8b8 |
| Source note | uspto-grants-1979_08 |