HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → Prop-2-enoic acid--2-ethylhexyl prop-2-enoate (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | Hydrogen iodide | HCID 24841 | — |
| Reactant | Quinine | HCID 3034034 | — |
| Solvent | 1-Decanol | HCID 8174 | — |
| Product | Prop-2-enoic acid--2-ethylhexyl prop-2-enoate (1/1) | HCID 168301 | — |
Reaction Steps
A copolymer of 2-ethylhexyl acrylate/acrylic acid, 50%/50% by weight was prepared. 42.5 grams of the solution of the copolymer was prepared as a 25% by weight solution in 2-ethoxyethanol to which was added 3.75 grams of quinine bisulphate and 8.50 grams of methanol. As in Example 1, an alcoholic solution of a plasticizer, iodine, and hydriodic acid was reacted with the above ingredients to form a wet paste. The dried paste, using heat to aid dispersion, was then suspended in decyl alcohol. The substance was placed in a light valve and satisfactory operation was achieved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04164365 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-7ab4e7344ee647d68253576063768233 |
| Source note | uspto-grants-1979_08 |