HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 20395264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 4-Methyl-3,4-dihydro-2H-1,4-benzoxazine-2-carboxylic acid | HCID 10845449 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20395264 | HCID 20395264 | — |
Reaction Steps
A solution of 1.1 g of 2A, and 5 ml of 2-propenamine in 25 ml of ethanol was refluxed for 16 hours. The solvent and excess amine were stripped off and the residue was passed through a silica gel column using Solvent No. 3 as eluent. The solvent was stripped off to give 2, as light yellow liquid, boiling point not determined.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04164576 |
| Source dataset | uspto-grants-1979_08 |
| ORD ID | ord-5c4d0229bff84cfbaa7e42bab1cec11c |
| Source note | uspto-grants-1979_08 |